Reactor X
High-temperature attachment for reactive gases
Reactor X allows measurements to be performed under high temperature (RT to 1,000°C) in air, inert gas or a mixture of these. Infrared heating allows rapid heating and cooling of samples. The sample stage and the sample holder are made of SiO₂, which allow measurements in various ambient environments.
The sample section can be separated from the furnace body, allowing sample setup or replacement inside the glove box. The heating rate is fast, up to 300°C/min, and measurements with good holding characteristics are also possible.
Reactor X Features
Reactor X Specifications
| Angle measurement range | θ=3°~83° (Aperture angle -2°~83°) | |
|---|---|---|
| Measurement optical system | Reflection method | |
| X-ray window material and thickness | Beryllium metal, 0.2 mm | |
| Operating temperature range | Room temperature to 1000℃ | |
| Sample atmosphere | Air, inert gas | |
| Temperature measuring thermocouple | K-type thermocouple (chromel - alumel) (Inconel sheath, also used for temperature measurement) | |
| Temperature stability | ±2℃ | |
| Sample heating method | Infrared heating | |
| Heating rate | 1～300℃/min | |
| Sample observation | Sample observation window | |
| Sample chamber | Sample section separation mechanism, compatible with glove boxes | |
| Cooling rate | 1000℃→100℃ within 6 minutes | |
Reactor X Application Notes
The following application notes are relevant to this product
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B-XRD1136 - Structural Characterization of Zeolite by Electron Density Analysis
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B-XRD1117 - Observation of a Phase Transition at High Temperature under Various Atmospheres
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B-XRD1078 - Evaluation of Crystallite Size and Pore Size distribution of Fuel Cell Materials
Reactor X Resources
Publications
| Saw-Tooth Heat-Cycling Nitridation of Metallic Cu Yields First Photoactive p-Cu₃N for PEC Applications | Read the Article |
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