CrysAlisPro Tip

How To Set Up Variable Temperature Measurements 

In this tutorial, learn how to set up and run a variable temperature measurement series using CrysAlisᴾʳᵒ. This step-by-step walkthrough covers everything from crystal mounting and centering to strategy setup and automated data collection across multiple temperature points.

You’ll see how to:

  • Mount and precisely center your crystal using the goniometer
  • Perform screening to evaluate crystal quality and unit cell parameters
  • Run a pre-experiment and generate data collection strategies
  • Create multiple measurement strategies for different symmetry conditions
  • Configure automated temperature steps and measurement sequences
  • Export and reuse experiment setups for efficiency
  • Monitor, stop, and resume multi-step experiments This guide is perfect for crystallographers and researchers who want to streamline temperature-dependent studies and improve experiment reproducibility using CrysAlisᴾʳᵒ. 

Presenter

Photo of Jakub Wojciechowski, PhD
Jakub Wojciechowski, PhD | Sr. Application Specialist Sales (SCX)

Rigaku Europe SE (RESE) | Neu-Isenburg by Frankfurt am Main, Germany

Dr. Jakub Wojciechowski is an application scientist working in the Rigaku Europe SE office based in Germany. Before Jakub joined Rigaku, he spent seven years as a crystallographer, research scientist and lecturer at the Łódź University of Technology in, Łódź, Poland. During this period, Jakub regularly collaborated with synthetic chemists, very often providing crucial information for publications, which is absolute structure results. Jakub is now responsible for supporting Rigaku’s clients in the Europe/Middle East/Africa region, helping them with data collection and processing, and also crystal structure publication. Want to learn more? Connect with Jakub Wojciechowski, PhD LinkedIn .

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