CrysAlisPro Tip
Frame Masking Tools
What is the issue?
Certain areas of diffraction images can sometimes be masked to improve data analysis. Diffraction images from high-pressure experiments may exhibit features of the diamond anvil or the gasket material, which could hamper determination of the unit cell. Another case is when area detectors exhibit untreated bad pixels, which may happen, for example, in foreign datasets from synchrotrons.
How to apply masks
CrysAlisPro allows you to mask rectangular features and ring-based (d-value) features.
Rectangular features:
Drag a box around the feature you want to mask with your mouse by holding down the left mouse button. Click on the right mouse button and select Reject rectangle.
This feature can be used for single images (choose run and frame number) or for the whole dataset (choose run and frame number as zeros).
The masked area can be displayed by choosing Show reject rectangle in the submenu next to the RED/USER switch.
Ring-based features:
First select the Line select (for skip d-value) via a right mouse button click.
Then the range of d-values which should be excluded from data analysis can be selected on the diffraction image. Click the right mouse button and select Skip d-value.
The masked area can be displayed by choosing Skip d-value overlay in the submenu of RED/USER as before.
Author

Rigaku Europe SE | Germany
Dr. Christian Göb is working as an application scientist for Rigaku Europe SE. He obtained his doctorate in supramolecular chemistry from the RWTH Aachen University (Germany) and worked as a visiting scientist at the Graduate School of Engineering Science, Osaka University (Japan). His expertise lies in application and characterization of large assemblies like molecular cages, their inclusion compounds and polymers (two-dimensional networks, metal and covalent organic frameworks). His main responsibilities include demonstrations and trainings for users of single crystal diffraction instruments, assistance in crystallographic questions, preparation of publication material and application of the crystalline sponge method in the EMEA region. Want to learn more? Connect with Christian Göb, PhD LinkedIn .

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