DicifferX WAXS Edition

Wide-angle X-ray scattering (WAXS) system

Revealing the structures of polymer materials

With DicifferX WAXS Edition, structural information that defines the properties of a wide range of materials—including polymer films, fibers, functional thin films, and lipids—can be obtained non-destructively, from atomic and molecular arrangements to crystal structures and molecular orientations. 

By focusing an intense X-ray beam into a fine spot with a high-brilliance rotating anode source and a multilayer X-ray focusing mirror, WE delivers rapid, high-precision measurements even on the smallest samples. Exposure time is reduced to just a few seconds, enabling time-resolved in-situ experiments under heating, stretching, humidity, and other conditions. The spacious stage, designed without a goniometer, allows direct mounting of large films, sheets, and multi-sample holders with ease.

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DicifferX WAXS Edition Overview

High-intensity micro X-ray beam for unmatched speed

By combining a high-intensity rotating anode X-ray generator with a high-precision multilayer focusing mirror, the system achieves an X-ray intensity of 10⁹ cps with a 200 μm beam width, directing a high-brilliance beam onto the sample.

The high-brilliance X-ray beam not only shortens measurement time significantly but also enhances time resolution. This enables high-speed time-resolved measurements that capture structural changes over time, such as during isothermal stretching of film materials.

Goniometer-free design for a spacious sample area and flexible attachments

The sample space, measuring 420 mm (H) × 190 mm (W) × 400 mm (D) with a load capacity of 5 kg, provides ample room for a wide variety of environmental stages and attachments. Linkam stretching and heating/cooling stages can also be controlled directly through Rigaku’s software, ensuring flexible adaptation to diverse sample environments and measurement needs.

Extended measurement capabilities for 2D data over a wide 2θ range (up to 360°)

The distance between the sample and the detector can be adjusted within a range of 40 to 140 mm. In two-dimensional flat-plate measurements, the system also supports coverage over a full 360° in the β direction.

Unique polymer structure analysis software

Rigaku’s proprietary software, specialized for polymer structure analysis, enables quantitative analysis of key information related to the properties of polymer materials—such as crystal structures and orientation distributions—using two-dimensional data, and provides clear visual representations of the results.

DicifferX WAXS Edition Features

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Fast, high-precision measurements
The high-brilliance X-ray beam shortens measurement time, enabling rapid feedback of results and wide-area mapping measurements in a short time.
High-speed time-resolved measurements in a lab environment
With exceptionally high time resolution, the system enables high-speed time-resolved measurements in a lab environment, such as during isothermal stretching of film materials.
Highly flexible sample space and measurement environment
The spacious sample area and high load capacity allow installation of a wide variety of environmental stages and attachments, including Linkam stretching and heating/cooling stages. This enables measurements of samples in diverse sizes and shapes.
Full Debye ring coverage
In addition to the wide selectable measurement area enabled by the detector’s large movable range, the extended measurement function—stitching multiple measurement images into a large-area image—makes it possible to perform two-dimensional measurements across the entire Debye ring.
Intuitive visualization of crystal orientation and more
With the polymer structure analysis software PolyOrientX, parameters such as orientation distribution and crystallite size can be used to compare measured data with simulation results. In addition, two-dimensional data can be utilized to visualize crystal structures, orientation distributions, and other features.

DicifferX WAXS Edition Specifications

Technique Wide-angle X-ray scattering (WAXS)
Applications Wide-angle X-ray scattering, GI-WAXS, crystallinity evaluation, orientation analysis, in-situ/operando measurements
Technology Optics optimized for two-dimensional wide-angle X-ray scattering measurements
Main components 1.2 kW rotating anode X-ray generator (MicroMax-007), VariMax mirror, high-energy resolution 2D hybrid pixel array detector (HyPix)
Options Sample attachments, cells, stages, others
Control (PC) External PC, MS Windows OS, DicifferX Guidance control software
Dimensions
(main unit)
1,450 (W) x 1,850 (H) x 1,100 (D)
Weight
(main unit)
Approx. 750 kg
Power supply Three-phase 200 V, 50/60 Hz, 20 A

DicifferX WAXS Edition Options

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