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Pharmalytical Summit 2021
Drug Preformulation

 

Building Quantitative XRF Methods on the ZSX Primus IV for Pharmaceuticals

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A brief discussion of the principles of XRF and demonstrate how a calibration is built and stored for a pharmaceutical material. Demonstration of how various sample types are analyzed using saved quantitative calibration methods.

Direct CNOX analysis of solid forms for confirmation of composition and determination of salts/stoichiometry, hydrates, and solvates by WDXRF

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Quantitative analysis of CNOX is achievable through WD-XRF using <100mg of retrievable sample. Accurate, rapid determination of CNO and other elements in API’s aids the chemist in solid form characterization such as solvates, salts, and hydrate stoichiometric determination.

Polymorph Monitoring Using 1064 nm Handheld Raman presented by Suzanne Schreyer, Ph.D.

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Polymorphs Throughout the Pharmaceutical Development Lifecycle - A Roundtable Discussion

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The speakers participating in this discussion are:

  • Ann Newman Ph.D. - Seventh Street Development Group
  • Steve Byrn, Ph.D. - Improved Pharma, LLC
  • Raj Suryanarayanan, Ph.D. - University of Minnesota
  • Mansoor Khan, Ph.D., RPh - Texas A&M College of Pharmacy
  • Eyal Barash - Barash Law LLC
  • Ken Morris, Ph.D. - Emeritus Long Island University and Hawaii University Hilo

Powder X-ray Diffraction (XRD) for Pharmaceuticals

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Powder X-ray Diffraction has diverse applications in the field of pharmaceutical sciences. This presentation summarizes significant achievements of the benchtop XRD instrument MiniFlex, multipurpose floor type XRD instrument SmartLab system for the solid forms phase analysis, crystallinity determination, cluster analysis, indexing and structure determination. Additionally, ease of configurational changes and auto alignment in both reflection and transmission geometry will be demonstrated. 

Use of Low-Frequency Raman Spectroscopy to Differentiate Almost Isoenergetic Polymorphs

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