- Customized X-ray system specifically tailored to the needs of your research.
- Faster, accurate data collection due to high-speed kappa goniometer, high-flux rotating anode X-ray source, fast, low-noise X-ray detector, and highly optimized instrument control software.
- Improve your ability to investigate small samples due to the increased flux from the rotating anode X-ray source as well as the extreme low noise of the HyPix X-ray detectors. Noise free images mean you can count longer for weakly diffracting crystals without a loss in data quality arising from detector noise.
- Increased data collection speed due to the increased flux of the X-ray source.
- Enhance your ability to resolve large unit cells, twins or incommensurate lattices when you select the optional motorized variable beam slit in order to alter divergence to adapt the source to your sample’s requirements.
Customized Single Crystal Diffraction System With Microfocus Rotating Anode Generator
X-ray crystal structure determination for advanced chemical crystallography
XtaLAB Synergy Custom
One of the advantages of Rigaku's rotating anode X-ray generators is the ability to utilize both ports of the generator simultaneously. This might involve having two single crystal goniometers mounted on the generator or it might involve having one goniometer with a sample changing robot on one port dedicated to protein crystallography and a second goniometer dedicated to chemical crystallography. In order to accommodate the various configurations that a researcher might envision, Rigaku offers the XtaLAB Synergy Custom, a system that can be configured with either a MicroMax-007 HF microfocus rotating anode source or the highest-flux in-house X-ray source, the FR-X. Additionally, the XtaLAB Synergy Custom comes in a specially designed enclosure with your choice of table size to accommodate accessory equipment, such as an ACTOR robotic system or a microscope close to the goniometer. Thus, the versatility offered by the XtaLAB Synergy Custom system provides the most flexibility possible for your structural chemistry program.
HPC direct detection X-ray detector
XtaLAB Synergy Custom systems are configured with a Hybrid Photon Counting (HPC) X-ray detector, such as the HyPix-6000HE, or the HyPix-Arc 150°. HPC detectors are ideal for difficult single crystal experiments because they are photon counting detectors that directly detect X-ray photons without the need for the intermediate step of converting X-ray photons to light with a phosphor or scintillator. As a result, HPCs have high dynamic range, fast readout speed and extremely low noise. Additionally, HPC X-ray detectors have a top-hat point spread function of a single pixel. These combined features, along with shutterless data collection, mean that you can collect more accurate diffraction data, faster. As a result, the XtaLAB Synergy Custom systems offer outstanding performance for demanding single crystal X-ray diffraction experiments.
The XtaLAB Synergy-Custom comes complete with CrysAlisPro, our user-inspired data collection and data processing software for single crystal analysis. Designed around an easy-to-use graphical user interface, CrysAlisPro can be operated under fully automatic, semi-automatic or manual control. CrysAlisPro combines automated crystal screening, the fastest and most accurate strategy software available, concurrent data reduction and automatic small molecule structure solution. Visual feedback is provided for each step with clear, color-coded guidance so that both novices and experts can collect high-quality data in the shortest time possible.
AutoChem is the ultimate productivity tool for small molecule chemists, offering fast, fully automatic structure solution and refinement during data collection. Developed in collaboration with OlexSys Ltd (Durham University, UK), AutoChem works in conjunction with Olex² where more advanced structure solution and refinement functionality exists. AutoChem is seamlessly integrated within CrysAlisPro, and forms an integral part of our ‘What is this?’ feature. The ‘What is this?’ feature gives you structures quickly and ensures you are not wasting time collecting full datasets on known samples or starting materials. It is an alternative pre-experiment option, which is used to plan your full data collections.
|Product name||XtaLAB Synergy Custom|
|Core attributes||X-ray diffractometer with dual port rotating anode X-ray source and HPC detector|
|Detectors||HyPix-6000HE or the large theta coverage HyPix-Arc 150°.|
|X-ray Source||MicroMax-007 HF microfocus rotating anode source or the highest-flux in-house X-ray source, the FR-X (Mo, Cu, or Ag).|
|Goniometer||Fast kappa geometry goniometer that allows data collection scan speeds of up to 10°/sec.|
|Accessories||Oxford Cryostream 800, Oxford Cobra, XtalCheck-S, High Pressure Kit, and Element Analyzer, ACTOR robotic sample changer|
|Computer||External PC, MS Windows® OS|
|Core dimensions||Varies with configuration|
|Mass||Varies with configuration|
|Power requirements||Varies with configuration|
The HyPix-Arc 150° is an optional, unique curved Hybrid Photon Counting (HPC) X-ray detector for single crystal diffraction applications.
The 800 Series Cryostream is the most robust, efficient and user-friendly liquid nitrogen based low temperature system available today. Specific features include a superior laminar flow system, meaning virtually zero risk of icing, extremely quiet running and a fast-start system resulting in a cool-down time to 100K of just 20 minutes.
The Oxford Cobra is the non-liquid nitrogen Cryostream. Combining the efficiency of a Cryostream with the advantages of a non-liquid system, the Cobra offers the ultimate solution for both macromolecular and small molecule crystallography.
The XtalCheck-S system includes software that facilitates both visual and diffraction imaging of crystallization experiments. With the XtalCheck-S system, one can easily survey many crystallization experiments by eliminating the need to harvest and cryo-cool samples. Moreover, one can perform serial crystallography experiments, by collecting data from multiple crystals, to achieve complete data sets that can be used for structure solution, as well as perform powder data collection from samples mounted in the crystallization wells.
Accommodating the vast majority of commercially available and custom high pressure cells the high pressure kit creates a sample space with an 8 cm diameter. It’s easy to switch between high pressure and standard mode and with powerful high-pressure software tools to aid with data analysis and processing, high pressure diffraction experiments have never been easier.
*Please check with your local sales person if your DAC is supported
The ELement ANalyzer is a state-of-the-art attachment that allows us to obtain qualitative information on elements in a single crystal at the same time as X-ray diffraction data collection for a single crystal structural analysis. By measuring the X-ray fluorescence spectrum emitted during X-ray diffraction experiments with the ELement ANalyzer, it becomes possible to perform elemental analysis on a single grain of crystal. The ELement ANalyzer can be used for confirmation the presence of central metal(s) in a mononuclear or polynuclear complex or solvent in a crystal for small molecule X-ray crystallography. There is a broad range of possible applications of the ELement ANalyzer in scientific fields.